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AE ject No. P-0025977 acre Page B 26 of 41 Pace Analytical Services, LLC 1700 Elm Street Minneapolis, MN 55414 (612)607-1700 ANALYTICAL RESULTS Project: P-0025977 Rolling Hills Pond Pace Project No.: 10669893 Sample: 136-A Lab ID: 10669893011 Collected: 09/21/23 12:00 Received: 09/22/23 11:31 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010D MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis Arsenic 3.1 mg/kg 1.1 1 09/27/2312:55 10/02/2314:00 7440-38-2 Copper 17.2 mg/kg 0.55 1 09/27/2312:55 10/02/2314:00 7440-50-8 Dry Weight 1 %M byASTM D2974 Analytical Method: ASTM D2974 Pace Analytical Services - Minneapolis Percent Moisture 16.4 % 0.10 1 10/03/23 15:48 8270E MSSV PAH by SIM Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 Pace Analytical Services - Minneapolis Acenaphthene ND ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 83-32-9 Acenaphthylene 20.6 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 208-96-8 Anthracene 32.6 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 120-12-7 Benzo(a)anthracene 110 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 56-55-3 Benzo(a)pyrene 174 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 50-32-8 Benzo(b)fluoranthene 296 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 205-99-2 Benzo(g,h,i)perylene 247 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 191-24-2 Benzo(k)fluoranthene 96.8 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 207-08-9 Chrysene 166 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 218-01-9 Dibenz(a,h)anthracene 53.6 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 53-70-3 Fluoranthene 291 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 206-44-0 Fluorene ND ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 86-73-7 Indeno(1,2,3-cd)pyrene 276 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 193-39-5 Naphthalene ND ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 91-20-3 Phenanthrene 81.0 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 85-01-8 Pyrene 190 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 129-00-0 Total BaP Eq. MN 2006sh. ND=O 284 ug/kg 11.9 1 09/27/23 08:35 09/29/23 03:10 Surrogates 2-Fluorobiphenyl (S) 81 %. 54-125 1 09/27/23 08:35 09/29/23 03:10 321-60-8 p-Terphenyl-d14 (S) 87 %. 60-125 1 09/27/23 08:35 09/29/23 03:10 1718-51-0 8270E MSSV CPAH by SIM Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 Pace Analytical Services - Minneapolis Acenaphthene ND ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 83-32-9 Acenaphthylene 19.5 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 208-96-8 Anthracene 18.0 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 120-12-7 Benzo(a)anthracene 105 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 56-55-3 Benzo(a)pyrene 152 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 50-32-8 Benzo(e)pyrene 173 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 192-97-2 Benzo(g,h,i)perylene 183 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 191-24-2 Benzofluoranthenes (Total) 349 ug/kg 35.5 1 09/28/23 18:14 10/02/23 21:13 Carbazole 18.9 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 86-74-8 2-Chloronaphthalene ND ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 91-58-7 Chrysene 186 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 218-01-9 Dibenz(a,h)acridine 13.3 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 226-36-8 Dibenz(a,h)anthracene 38.2 ug/kg 11.8 1 09/28/23 18:14 10/02/23 21:13 53-70-3 REPORT OF LABORATORY ANALYSIS N2 10161 This report shall not be reproduced, except in full, Date: 10/05/2023 02:34 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 41