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AE ject No. P-0025977 acre Page B 18 of 41 Pace Analytical Services, LLC 1700 Elm Street Minneapolis, MN 55414 (612)607-1700 ANALYTICAL RESULTS Project: P-0025977 Rolling Hills Pond Pace Project No.: 10669893 Sample: 134-A Lab ID: 10669893007 Collected: 09/21/23 11:00 Received: 09/22/23 11:31 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010D MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis Arsenic 1.8 mg/kg 1.3 1 09/27/2312:55 10/02/2313:50 7440-38-2 Copper 13.5 mg/kg 0.63 1 09/27/2312:55 10/02/2313:50 7440-50-8 Dry Weight 1 %M byASTM D2974 Analytical Method: ASTM D2974 Pace Analytical Services - Minneapolis Percent Moisture 25.8 % 0.10 1 10/03/23 15:47 8270E MSSV PAH by SIM Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 Pace Analytical Services - Minneapolis Acenaphthene ND ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 83-32-9 Acenaphthylene ND ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 208-96-8 Anthracene ND ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 120-12-7 Benzo(a)anthracene 110 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 56-55-3 Benzo(a)pyrene 217 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 50-32-8 Benzo(b)fluoranthene 579 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 205-99-2 Benzo(g,h,i)perylene 335 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 191-24-2 Benzo(k)fluoranthene 167 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 207-08-9 Chrysene 240 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 218-01-9 Dibenz(a,h)anthracene 79.1 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 53-70-3 Fluoranthene 308 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 206-44-0 Fluorene ND ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 86-73-7 Indeno(1,2,3-cd)pyrene 432 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 193-39-5 Naphthalene ND ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 91-20-3 Phenanthrene 57.2 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 85-01-8 Pyrene 197 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 129-00-0 Total BaP Eq. MN 2006sh. ND=O 392 ug/kg 13.4 1 09/27/23 08:35 09/29/23 01:52 Surrogates 2-Fluorobiphenyl (S) 81 %. 54-125 1 09/27/23 08:35 09/29/23 01:52 321-60-8 p-Terphenyl-d14 (S) 83 %. 60-125 1 09/27/23 08:35 09/29/23 01:52 1718-51-0 8270E MSSV CPAH by SIM Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3546 Pace Analytical Services - Minneapolis Acenaphthene ND ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 83-32-9 Acenaphthylene ND ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 208-96-8 Anthracene ND ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 120-12-7 Benzo(a)anthracene 60.6 ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 56-55-3 Benzo(a)pyrene 151 ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 50-32-8 Benzo(e)pyrene 207 ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 192-97-2 Benzo(g,h,i)perylene 203 ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 191-24-2 Benzofluoranthenes (Total) 456 ug/kg 39.1 1 09/28/23 18:14 10/02/23 19:09 Carbazole 23.2 ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 86-74-8 2-Chloronaphthalene ND ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 91-58-7 Chrysene 192 ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 218-01-9 Dibenz(a,h)acridine 13.6 ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 226-36-8 Dibenz(a,h)anthracene 36.8 ug/kg 13.0 1 09/28/2318:14 10/02/2319:09 53-70-3 REPORT OF LABORATORY ANALYSIS N2 10161 This report shall not be reproduced, except in full, Date: 10/05/2023 02:34 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 41